1-氯-2,4-二硝基苯合成路线 （共 755 条）
参考文献
Michels, Theo D.; Rhee, Jong Uk; Vanderwal, Christopher D.
Organic Letters, 2008 , vol. 10, # 21 p. 4787 - 4790
反应条件
in 1,4-dioxane; water
T=45°C; 0.5 h; other temperatures; KineticsThermodynamic dataProduct distribution;
参考文献
Ikramuddeen; Chandrasekara; Ramarajan; Subramania n
Journal of the Indian Chemical Society, 1989 , vol. 66, # 5 p. 342 - 344
反应条件
1: alcohol; NaOH-solution
2: HNO3+H2SO4
View Scheme
参考文献
Marqueyrol; Scohy
Bulletin de la Societe Chimique de France, 1920 , vol. <4> 27, p. 105
参考文献
Dey; Doraiswami
Journal of the Indian Chemical Society, 1933 , vol. 10, p. 309,320
反应条件
ethanol
Behandeln einer wss. Loesung des Reaktionsprodukts mit wss. Schwefelsaeure;
参考文献
Fehnel; Amstutz
Industrial and Engineering Chemistry, Analytical Edition, 1944 , vol. 16, p. 53
参考文献
Benn et al.
Journal of the Chemical Society, 1958 , p. 2800,2804
反应条件
1.1: t-BuOK / 1-methyl-pyrrolidin-2-one; dioxane / 20 - 70 °C
1.2: 1-methyl-pyrrolidin-2-one; dioxane / 70 °C
1.3: HCl / dioxane
2.1: Fe; AcOH / 1-methyl-pyrrolidin-2-one; dioxane / 3 h / 85 °C
3.1: 0.79 g / NaOH / methanol / 6 h / Heating
View Scheme
参考文献
Gallou, Fabrice; Yee, Nathan; Qiu, Fenghe; Senanayake, Chris; Linz, Guenter; Schnaubelt, Juergen; Soyka, Rainer
Synlett, 2004 , # 5 p. 883 - 885
反应条件
sodium methylate in methanol
参考文献
Machacek, Vladimir; Sterba, Vojeslav; Kolb, Ivan; Lycka, Antonin
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 5 p. 1044 - 1052
反应条件
platinum on charcoal; sulfided; vanadium pentoxide in water
T=91 - 95°C; Product distribution / selectivity;
参考文献
LONZA AG
Patent: WO2004/74234 A1, 2004 ;
Location in patent: Page 5 ;
反应条件
1: ethanol
2: ethanol; aqueous sodium polysulfide
View Scheme
参考文献
Saunders
Journal of the Chemical Society, 1955 , p. 3275,3282
