1-氯-2,4-二硝基苯合成路线 （共 755 条）
反应条件
methanol; potassium hydroxide
参考文献
Yoneda
Yakugaku Zasshi, 1957 , vol. 77, p. 944
Chem.Abstr., 1958 , p. 2855
反应条件
sodium carbonate in acetone
Substitution; 5 h; Heating;
参考文献
Gierczyk; Leska; Nowak-Wydra; Schroeder; Wojciechowski; Bartl; Brzezinski
Journal of Molecular Structure, 2000 , vol. 524, # 1-3 p. 217 - 225
参考文献
Dupas, G.; Decormeille, A.; Bourguignon, J.; Queguiner, G.
Tetrahedron, 1989 , vol. 45, # 9 p. 2579 - 2590
参考文献
University of Florida
Patent: US4963682 A1, 1990 ;
反应条件
1: in ethanol
T=40°C; 24 h; Heating / reflux;
2: With ammonia in ethanol; water
T=20°C; pH=10 - 11;
参考文献
Renton, Paul; Green, Brenda; Maddaford, Shawn; Rakhit, Suman; Andrews, John S.
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 3 p. 227 - 231
反应条件
1: ethanol
2: phosphorus (III)-chloride; chloroform
3: benzene / 120 °C
View Scheme
参考文献
Hippchen
Chemische Berichte, 1947 , vol. 80, p. 263,270
参考文献
Gupta,S.P.; Dureja,P.
Journal of the Indian Chemical Society, 1973 , vol. 50, p. 546 - 548
反应条件
sulfuric acid; bromine; nitric acid
T=80 - 85°C;
参考文献
Andrievskii, A.M.; Gorelik, M.V.; Avidon, S.V.; Al'tman, E.Sh.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 9.2 p. 1519 - 1524
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 9 p. 1828 - 1834
反应条件
1: 32 g / NH3, Al(OAc)3 / 6 h / 170 °C
2: 1.) NaNO2, H2SO4, 2.) H2SO4, NaOAc, glacial AcOH / 1.) 10 deg C, 2.) 5 deg C, overnight
View Scheme
参考文献
Johri; Varshney
Journal of the Indian Chemical Society, 1996 , vol. 73, # 11 p. 629 - 630
反应条件
carbon disulfide; sodium hydrogensulfide
参考文献
Teppema; Sebrell
Journal of the American Chemical Society, 1927 , vol. 49, p. 1757
