甲基α-D-吡喃葡萄糖苷合成路线 （共 276 条）
反应条件
sodium hydride in N,N-dimethyl-formamide T=75°C; 24 h;
参考文献
Zhang, Guang-Tao; Guo, Zhong-Wu; Hui, Yong-Zheng
Synthetic Communications, 1997 , vol. 27, # 11 p. 1907 - 1917
反应条件
trifluorormethanesulfonic acid in 1,4-dioxane T=20°C; 2 h; Inert atmosphere;
参考文献
Yamada, Kohei; Fujita, Hikaru; Kunishima, Munetaka
Organic Letters, 2012 , vol. 14, # 19 p. 5026 - 5029,4
Title/Abstract Full Text Show Details
Yamada, Kohei; Fujita, Hikaru; Kunishima, Munetaka
Organic Letters, 2012 , vol. 14, # 19 p. 5026 - 5029
反应条件
potassium hydroxide; potassium carbonate T=120°C; 1 h; Further byproducts.;
参考文献
Synthetic Communications, , vol. 37, # 13 p. 2195 - 2202
反应条件
1: methyl D-glucopyranoside With sodium hydride in N,N-dimethyl-formamide; mineral oil T=0°C; 0.5 h; 2: benzyl bromide in N,N-dimethyl-formamide; mineral oil T=0 - 20°C;
参考文献
Fernandez-Herrera, Maria A.; Mohan, Sankar; Lopez-Munoz, Hugo; Hernandez-Vazquez, Jose M.V.; Perez-Cervantes, Esmeralda; Escobar-Sanchez, Maria L.; Sanchez-Sanchez, Luis; Regla, Ignacio; Pinto, B. Mario; Sandoval-Ramirez, Jesus
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 11 p. 4827 - 4837
反应条件
potassium hydroxide T=120°C; 3 h; Further byproducts.;
参考文献
Synthetic Communications, , vol. 37, # 13 p. 2195 - 2202
参考文献
Yang, Bing-Hui
Tetrahedron Letters, 1995 , vol. 36, # 16 p. 2831 - 2834
反应条件
water; oxygen; sodium hydrogencarbonate in Gegenwart von Platin und Erhitzen des Reaktionsprodukts mit wasserhaltiger Ameisensaeure;
参考文献
Corn Prod. Refining Co.
Patent: US2683150 , 1950 ;
反应条件
bis(tri-n-butyltin)oxide 1.) toluene, reflux, 5 h, 2.) toluene, 50 deg C, 70 h; Yield given. Multistep reaction;
参考文献
Ogawa, Tomoya; Matsui, Masanao
Tetrahedron, 1981 , vol. 37, p. 2363 - 2370
反应条件
1: 73 percent / CBr4, Ph3P / acetonitrile / 36 h / Ambient temperature 2: 15 percent / 1,2-dichloro-ethane / 24 h / Heating View Scheme
参考文献
Cicero, Daniel; Varela, Oscar; De Lederkremer, Rosa M.
Tetrahedron, 1990 , vol. 46, # 4 p. 1131 - 1144
反应条件
sodium hydride in N,N-dimethyl-formamide T=20°C; Substitution; 2.5 h;
参考文献
Wang, Wei; Zhang, Yongmin; Sollogoub, Matthieu; Sinay, Pierre
Angewandte Chemie (International Edition in English), 2000 , vol. 39, # 14 p. X2466-2467
