甲基α-D-吡喃葡萄糖苷合成路线 (共 276 条)
反应条件
iron(III) chloride T=28 - 32°C; 36 h;
参考文献
Dasgupta, Falguni; Singh, Prem P.; Srivastava, Harish H.
Carbohydrate Research, 1980 , vol. 80, p. 346 - 349
反应条件
iron(III) chloride T=60°C; 3 h; other carbohydrates, other reaction times;
参考文献
Dasgupta, Falguni; Singh, Prem P.; Srivastava, Harish C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 527 - 529
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; trichloroisocyanuric acid; sodium hydrogencarbonate in N,N-dimethyl-formamide T=0°C; 7 h;
参考文献
Angelin, Marcus; Hermansson, Magnus; Dong, Hai; Ramstrom, Olof
European Journal of Organic Chemistry, 2006 , # 19 p. 4323 - 4326
反应条件
sulfuric acid; 4-acetylamino 2,2,6,6-tetramethylpiperidin-N-oxyl in water T=20°C; pH=0.5 - 1.5; 48 h;
参考文献
SCA Hygiene Products Zeist B.V.
Patent: US6936710 B2, 2005 ;
Location in patent: Page/Page column 3 ;
反应条件
oxygen; platinum on activated charcoal in water T=49.9°C; P=300.02 Torr; initial rate of consumption, pH effect; Product distributionMechanism;
参考文献
Vleeming, Johannes H.; Kuster, Ben F.M.; Marin, Guy B.
Carbohydrate Research, 1997 , vol. 303, # 2 p. 175 - 183
反应条件
1: imidazole; triphenylphosphine; iodine / toluene / 2.5 h / Heating 2: pyridine / 12 h 3: sulphuric acid / 12 h / 20 °C View Scheme
参考文献
Miller, Justin N.; Pongdee, Rongson
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3185 - 3187
反应条件
1: 75 percent / ZnCl2 / CHCl3 2: 1.) Bu2SnO, 2.) Et3N / 1.) MeOH, benzene, reflux, 2.) 10 deg C to RT View Scheme
参考文献
Joseph, A. Abragam; Verma, Ved Prakash; Liu, Xin-Yi; Wu, Chia-Hui; Dhurandhare, Vijay M.; Wang, Cheng-Chung
European Journal of Organic Chemistry, 2012 , # 4 p. 744 - 753
反应条件
oxygen; platinum on activated charcoal in water T=49.9°C; P=300.02 Torr; initial rate of consumption, pH effect; Product distributionMechanism;
参考文献
Vleeming, Johannes H.; Kuster, Ben F.M.; Marin, Guy B.
Carbohydrate Research, 1997 , vol. 303, # 2 p. 175 - 183
参考文献
Bergmann; Wolff
Chemische Berichte, 1923 , vol. 56, p. 1060,1064
反应条件
pyridinium p-toluenesulfonate in N,N-dimethyl-formamide
参考文献
Tatina, Madhubabu; Yousuf, Syed Khalid; Mukherjee, Debaraj
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 28 p. 5357 - 5360