甲基α-D-吡喃葡萄糖苷合成路线 (共 276 条)
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=20°C; 0.166667 h; Inert atmosphere;
参考文献
Joseph, A. Abragam; Verma, Ved Prakash; Liu, Xin-Yi; Wu, Chia-Hui; Dhurandhare, Vijay M.; Wang, Cheng-Chung
European Journal of Organic Chemistry, 2012 , # 4 p. 744 - 753
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran Ambient temperature;
参考文献
Johnson
Carbohydrate Research, 1992 , vol. 237, p. 313 - 318
反应条件
in N,N-dimethyl-formamide T=100°C; 0.0833333 h;
参考文献
Mai, Khuong; Patil, Ghanshyam
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3545 - 3548
反应条件
in acetonitrile T=78 - 80°C; 3 h;
参考文献
Bennek, John A.; Gray, Gary R.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 892 - 897
反应条件
iron(III) chloride T=60°C; 3 h; other carbohydrates, other reaction times;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 27, # 1-12 p. 527 - 529
反应条件
water T=350°C; 0.0333333 h; hydrothermolysis of several carbohydrates, various temperature; Product distribution;
参考文献
Kallury, R. Krishna M. R.; Ambidge, Chris; Tidwell, Thomas T.; Boocock, David G. B.; Agblevor, Foster A.; Stewart, Daniel J.
Carbohydrate Research, 1986 , vol. 158, p. 253 - 261
反应条件
1: 83 percent / camphor sulfonic acid / dimethylformamide / 60 °C / 180.01 Torr 2: 77 percent / pyridine / CH2Cl2 / 3 h / -30 °C 3: 83 percent / tetra-n-butylammonium iodide / toluene / 4 h / 80 °C 4: 69 percent / Zn; H2PtCl6; AcOH / CH2Cl2 / 1 h View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 14, # 13 p. 1767 - 1769
反应条件
sodium hydride in N,N-dimethyl-formamide T=20°C; Substitution; 2.5 h;
参考文献
Wang, Wei; Zhang, Yongmin; Sollogoub, Matthieu; Sinay, Pierre
Angewandte Chemie (International Edition in English), 2000 , vol. 39, # 14 p. X2466-2467
反应条件
sodium hydride in N,N-dimethyl-formamide T=75°C; 24 h;
参考文献
Zhang, Guang-Tao; Guo, Zhong-Wu; Hui, Yong-Zheng
Synthetic Communications, 1997 , vol. 27, # 11 p. 1907 - 1917
反应条件
trifluorormethanesulfonic acid in 1,4-dioxane T=20°C; 2 h; Inert atmosphere;
参考文献
Yamada, Kohei; Fujita, Hikaru; Kunishima, Munetaka
Organic Letters, 2012 , vol. 14, # 19 p. 5026 - 5029,4
Title/Abstract Full Text Show Details
Yamada, Kohei; Fujita, Hikaru; Kunishima, Munetaka
Organic Letters, 2012 , vol. 14, # 19 p. 5026 - 5029