甲基α-D-吡喃葡萄糖苷合成路线 (共 276 条)
反应条件
potassium hydroxide; potassium carbonate T=120°C; 1 h; Further byproducts.;
参考文献
Synthetic Communications, , vol. 37, # 13 p. 2195 - 2202
反应条件
1: methyl D-glucopyranoside With sodium hydride in N,N-dimethyl-formamide; mineral oil T=0°C; 0.5 h; 2: benzyl bromide in N,N-dimethyl-formamide; mineral oil T=0 - 20°C;
参考文献
Fernandez-Herrera, Maria A.; Mohan, Sankar; Lopez-Munoz, Hugo; Hernandez-Vazquez, Jose M.V.; Perez-Cervantes, Esmeralda; Escobar-Sanchez, Maria L.; Sanchez-Sanchez, Luis; Regla, Ignacio; Pinto, B. Mario; Sandoval-Ramirez, Jesus
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 11 p. 4827 - 4837
反应条件
potassium hydroxide T=120°C; 3 h; Further byproducts.;
参考文献
Synthetic Communications, , vol. 37, # 13 p. 2195 - 2202
参考文献
Yang, Bing-Hui
Tetrahedron Letters, 1995 , vol. 36, # 16 p. 2831 - 2834
反应条件
1: TsOH 2: pyridine / Ambient temperature View Scheme
参考文献
Chen, Xiaozhuo; Xu, Peng; Xu, Yanpeng; Liu, Lu; Liu, Yi; Zhu, Di; Lei, Pingsheng
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 24 p. 7402 - 7405
反应条件
1: DMAP / pyridine 2: KOH / 130 °C 3: ceric ammonium nitrate / H2O; acetonitrile View Scheme
参考文献
Pasti, Claudia; Rinaldi, Eliana; Cervellati, Carlo; Dallocchio, Franco; Hardre, Renaud; Salmon, Laurent; Hanau, Stefania
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 7 p. 1207 - 1214
反应条件
trityl chloride Multistep reaction;
参考文献
Ronchi, Paolo; Vignando, Stefano; Guglieri, Sara; Polito, Laura; Lay, Luigi
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 12 p. 2635 - 2644
反应条件
1: TsOH 2: pyridine / Ambient temperature View Scheme
参考文献
Chen, Xiaozhuo; Xu, Peng; Xu, Yanpeng; Liu, Lu; Liu, Yi; Zhu, Di; Lei, Pingsheng
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 24 p. 7402 - 7405
反应条件
sulfuric acid; acetic acid in water 6 h; Reflux;
参考文献
Li, Tiehai; Guo, Lina; Zhang, Yan; Wang, Jiajia; Zhang, Zhenxing; Li, Jing; Zhang, Wenpeng; Lin, Jianping; Zhao, Wei; Wang, Peng George
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 7 p. 2136 - 2144
反应条件
oxygen; platinum on activated charcoal in water T=49.9°C; P=300.02 Torr; initial rate of consumption, pH effect; Product distributionMechanism;
参考文献
Vleeming, Johannes H.; Kuster, Ben F.M.; Marin, Guy B.
Carbohydrate Research, 1997 , vol. 303, # 2 p. 175 - 183