1: methylenesuccinic acid With hydrogen; BINAP-RuCl2*dmf in methanol T=50°C; Catalytic hydrogenation; P=30002.4 Torr; 2: methanol With thionyl chloride Esterification; 2 h; Title compound not separated from byproducts;
参考文献
Ter Halle, Rob; Schulz, Emmanuelle; Spagnol, Michel; Lemaire, Marc
Tetrahedron Letters, 2000 , vol. 41, # 18 p. 3323 - 3326