in ethanol to a soln. of 0.11 g of the gold complex in EtOH is added a soln. of 0.06 g (Et2NC(S)S)2 in EtOH (20°C); the mixt. is stirred for 15 min; pptd. gold diethylthiocarbamate filtered off and washed with ether; mother liquor evapd. to dryness under vac., residue washed with benzene and recrystd. from alc.;
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Victoriano, Luis I.; Garland, Maria Teresa; Vega, Andres; Lopez, Cesar
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Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 4.2 p. 819 - 822
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 909 - 913
in chloroform Kinetics; Irradiation (UV/VIS); photochemical react. of copper powder with TETD in chloroform; product is filtered and recrystd. from chloroform; elem. anal.;
参考文献
Tetsumi, T.; Sumi, M.; Tanaka, M.; Shono, T.
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