in pentane byproducts: ethane; to cooled soln. of Et3Al added dropwise soln. of Et2BOH with vigorous stirring at 0-20°C, left to reach room temp.; distd. off in vac.;
参考文献
Journal of Organometallic Chemistry, , vol. 284, p. 1 - 4
in hexane N2-atmosphere; addn. of 2 equiv. AlEt3 to borane (-78°C), stirring (room temp., 20 h); not isolated, reaction followed by (11)B- and (27)Al-NMR spectroscopy;
参考文献
Journal of Organometallic Chemistry, , vol. 489, # 1-2 p. 51 - 62
