in benzene to a benzene soln. of AlEt3 was added dropwise a benzene soln. of 8-quinolinol for 1 h, the mixt. was stirred at room temp. for 3 h (inert atm.); ppt. was washed with benzene and dried in vac.; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 654, # 1-2 p. 229 - 232
1: triethylaluminum With titanium(IV) isopropylate; (S)-2-hydroxy-3-phenylpropionic acid in tetrahydrofuran; toluene T=20°C; 6 h; 2: 3-chloro-benzaldehyde in tetrahydrofuran; toluene T=20°C; 6 h; Title compound not separated from byproducts;
