反应条件
C2H5OH; HCl in further solvent(s) under N2, Ru complex suspended in Et3Al, mixt. stirred at 75°C for 2 h, mixt. cooled to -10°C, ethanol slowly added, stirred at room temp. for 3.5 h; solvent removed, residue dissolved in CH2Cl2, added concd. HCl, org. layer sepd., dried, recrystd. from CH2Cl2/ethanol;
参考文献
Grocott, Stephen C.; Wild, Stanley Bruce
Inorganic Chemistry, 1982 , vol. 21, p. 3526 - 3534