Zakharkin, L. I.; Okhlobystin, O. Yu.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1959 , p. 1942 - 1947
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Gmelin Handbook: Bi: Org.Verb., 1.3.3.1.1, page 46 - 55
in hexane
molar ratio of Al(C2H5)3 and Sb2O3 = 3 : 1, 60°C, 1 to 2 h; distn. in high vac.;
参考文献
Stamm,W.; Breindel,A.
Angewandte Chemie, 1964 , vol. 76, p. 99
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Stamm, W.
Trans. N. Y. Acad. Sci. (2), 1966 , vol. 28, p. 396 - 401
in neat (no solvent)
under N2; Al-compd. added slowly over a period of 2 h to Sb-compd. at 0°C with stirring, warmed slowly to room temp., stirred for 4 h, heated for 12 h at 120°C; monitored by NMR, fractional distn., Al-compd. isolated by distn.;;
参考文献
Thomas, C. J.; Krannich, L. K.; Watkins, C. L.
Polyhedron, 1993 , vol. 12, p. 89 - 94
