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in neat (no solvent) Sonication; (N2), ZnCl2 introduced into a flask connected to a condenser containingalcohol at -20°C, Et3Al (Et3Al/ZnCl2 2.2) dropped into flask over 10 min at room temp., stirred and heated at 100°C for 1 hed forfurther 20 min; distd.; NMR;
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Lin, Yih-tsung
Journal of Organometallic Chemistry, 1986 , vol. 317, p. 277 - 284
in hexane T=0°C; 30 h; different hydrolysis conditions; other α,β-unsaturated nitro compounds and triorganoaluminum compounds and their etherates; Product distribution;
参考文献
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