n-butyllithium in tetrahydrofuran; pentane byproducts: isobutylene; (N2); to stirred soln. of boranederiv. in THF was dropwise added pentane soln. of LiBu at -78°C, then mixt. was allowed to warm up to room temp.; not isolated, detected by (11)B-NMR;
参考文献
Brown, Herbert C.; Kramer, Gary W.; Hubbard, John L.; Krishnamurthy, S.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 1 p. 1 - 10
