反应条件
in hexane suspending Me2Sn(CCCH3)2 (0.25M) in hexane (100ml), addn. of Me2SnCl2 (0.288M) and 3h heating at 65°C; cooling down at -78°C, addn. of triethylborane (0.53M), warming up soln. first at room temp., then2h heating at 65°C;; removal of hexane and excess triethylborane in vacuum, distn. of ppt.;;
参考文献
Kerschl, Susanna; Wrackmeyer, Bernd
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1986 , vol. 41, # 7 p. 890 - 894
