反应条件
1: (1S,3S,4R)-2-benzyl-3-[(1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]-2-thioniabicyclo[2.2.1]heptane tetrafluoroborate With lithium hexamethyldisilazane in tetrahydrofuran; dichloromethane T=-78°C; 1 h; 2: triethyl borane in tetrahydrofuran; dichloromethane T=-100 - 0°C; 3: With hydroxylamine-o-sulphonic acid in tetrahydrofuran; dichloromethane T=0 - 20°C; Further stages.;
参考文献
Fang, Guang Y.; Wallner, Olov A.; Di Blasio, Nadia; Ginesta, Xavier; Harvey, Jeremy N.; Aggarwal, Varinder K.
Journal of the American Chemical Society, 2007 , vol. 129, # 47 p. 14632 - 14639
