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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
97235-08-0
合成路线
（共 14 条）
139338-95-7
→
反应条件
97235-08-0
反应条件
in various solvent(s) T=185°C; 36 h;
参考文献
Boger; Zhu
Tetrahedron Letters, 1991 , vol. 32, # 52 p. 7643 - 7646
Title/Abstract Full Text View citing articles Show Details
Boger; Ichikawa; Jiang
Journal of the American Chemical Society, 2000 , vol. 122, # 49 p. 12169 - 12173
18643-50-0
→
反应条件
97235-08-0
反应条件
1: 99 percent / PPTS / CH2Cl2 2: 99 percent / Bu4NF / tetrahydrofuran 3: 77 percent / PDC 4: 96 percent / NaH 5: 96 percent / pyridine 6: 96 percent / Amberlyst / methanol 7: 86 percent / (COCl)2; DMSO 8: 70 percent / various solvent(s) / 36 h / 185 °C View Scheme
参考文献
Boger; Ichikawa; Jiang
Journal of the American Chemical Society, 2000 , vol. 122, # 49 p. 12169 - 12173
139338-86-6
→
反应条件
97235-08-0
反应条件
1: 99 percent / PPTS / CH2Cl2 2: 99 percent / Bu4NF / tetrahydrofuran 3: 77 percent / PDC 4: 96 percent / NaH 5: 96 percent / pyridine 6: 96 percent / Amberlyst / methanol 7: 86 percent / (COCl)2; DMSO 8: 70 percent / various solvent(s) / 36 h / 185 °C View Scheme
参考文献
Boger; Ichikawa; Jiang
Journal of the American Chemical Society, 2000 , vol. 122, # 49 p. 12169 - 12173
139338-87-7
→
反应条件
97235-08-0
反应条件
1: 77 percent / PDC 2: 96 percent / NaH 3: 96 percent / pyridine 4: 96 percent / Amberlyst / methanol 5: 86 percent / (COCl)2; DMSO 6: 70 percent / various solvent(s) / 36 h / 185 °C View Scheme
参考文献
Boger; Ichikawa; Jiang
Journal of the American Chemical Society, 2000 , vol. 122, # 49 p. 12169 - 12173
139338-88-8
→
反应条件
97235-08-0
反应条件
1: 96 percent / NaH 2: 96 percent / pyridine 3: 96 percent / Amberlyst / methanol 4: 86 percent / (COCl)2; DMSO 5: 70 percent / various solvent(s) / 36 h / 185 °C View Scheme
参考文献
Boger; Ichikawa; Jiang
Journal of the American Chemical Society, 2000 , vol. 122, # 49 p. 12169 - 12173
139338-89-9
→
反应条件
97235-08-0
反应条件
1: 96 percent / pyridine 2: 96 percent / Amberlyst / methanol 3: 86 percent / (COCl)2; DMSO 4: 70 percent / various solvent(s) / 36 h / 185 °C View Scheme
参考文献
Boger; Ichikawa; Jiang
Journal of the American Chemical Society, 2000 , vol. 122, # 49 p. 12169 - 12173
139339-27-8
→
反应条件
97235-08-0
反应条件
1: 99 percent / Bu4NF / tetrahydrofuran 2: 77 percent / PDC 3: 96 percent / NaH 4: 96 percent / pyridine 5: 96 percent / Amberlyst / methanol 6: 86 percent / (COCl)2; DMSO 7: 70 percent / various solvent(s) / 36 h / 185 °C View Scheme
参考文献
Boger; Ichikawa; Jiang
Journal of the American Chemical Society, 2000 , vol. 122, # 49 p. 12169 - 12173
139338-92-4
→
反应条件
97235-08-0
反应条件
1: 86 percent / (COCl)2; DMSO 2: 70 percent / various solvent(s) / 36 h / 185 °C View Scheme
参考文献
Boger; Ichikawa; Jiang
Journal of the American Chemical Society, 2000 , vol. 122, # 49 p. 12169 - 12173
139338-94-6
→
反应条件
97235-08-0
反应条件
1: 95 percent / (COCl)2; DMSO 2: 70 percent / various solvent(s) / 36 h / 185 °C View Scheme
参考文献
Boger; Ichikawa; Jiang
Journal of the American Chemical Society, 2000 , vol. 122, # 49 p. 12169 - 12173
139360-50-2
→
反应条件
97235-08-0
反应条件
1: 96 percent / Amberlyst / methanol 2: 86 percent / (COCl)2; DMSO 3: 70 percent / various solvent(s) / 36 h / 185 °C View Scheme
参考文献
Boger; Ichikawa; Jiang
Journal of the American Chemical Society, 2000 , vol. 122, # 49 p. 12169 - 12173
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