quinoline; hydrogen; Pd-BaSO4 in methanol Ambient temperature;

1: 92 percent / H2(g), quinoline / 5percent Pd/BaSO4 / methanol / Ambient temperature 2: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 20 min 3: tetrahydrofuran / 0.33 h 4: 200 °C View Scheme

1: 92 percent / H2(g), quinoline / 5percent Pd/BaSO4 / methanol / Ambient temperature 2: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 20 min 3: tetrahydrofuran / 0.33 h 4: 200 °C View Scheme

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11342940', constants.ctx, '0')">sodium hydroxide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />1&nbsp;h;&nbsp;&nbsp;Ambient temperature;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: NaBr / acetonitrile; H₂O / 9 h / Ambient temperature; electrolysis<br />2: NaOH / acetonitrile; H₂O / 1 h / Ambient temperature<br /> <br /> &nbsp;