4,4''-二甲基-1,1':4',1''-三联苯合成路线 （共 42 条）
反应条件
Ni(PCy3)2Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=90°C; Negishi coupling reaction; 8 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Angewandte Chemie - International Edition, 2011 , vol. 50, # 21 p. 4901 - 4904
反应条件
C35H50I2N2O2PPd; caesium carbonate in 1,4-dioxane
T=110°C; Suzuki Coupling; 12 h; Inert atmosphere;
参考文献
Xu, Chen; Hao, Xin-Qi; Li, Zhen; Duan, Lu-Meng; Wang, Zhi-Qiang; Ji, Bao-Ming; Song, Mao-Ping
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 10 p. 3430 - 3432
反应条件
C35H31BrN4NiP in tetrahydrofuran
T=25°C; 13 h; Schlenk techniqueInert atmosphere;
参考文献
Guo, Wang-Jun; Wang, Zhong-Xia
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 1054 - 1061
反应条件
bis(acetylacetonate)nickel(II); IPr*HBF4 in tetrahydrofuran; diethyl ether
T=25°C; 1.5 h; Inert atmosphere;
参考文献
Jo, Hyunjong; Kim, Chul-Bae; Ryoo, Tae-Yong; Ahn, Bo-Kyoung; Park, Kwangyong
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 12 p. 3749 - 3754
反应条件
1: para-difluorobenzene; p-MeC6H4ZnCl With Ni(PCy3)2Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=25 - 100°C; 10 h; Schlenk techniqueInert atmosphere;
2: p-MeC6H4ZnCl in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=100°C; 10 h; Inert atmosphereSchlenk technique;
参考文献
Zhu, Feng; Wang, Zhong-Xia
Journal of Organic Chemistry, 2014 , vol. 79, # 10 p. 4285 - 4292
反应条件
C68H72Cl2N6NiP2 in toluene
T=120°C; 16 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Chemistry - A European Journal, 2011 , vol. 17, # 18 p. 4972 - 4975
反应条件
Ni(PCy3)2Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=90°C; Negishi coupling reaction; 8 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Angewandte Chemie - International Edition, 2011 , vol. 50, # 21 p. 4901 - 4904
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in tetrahydrofuran
30 h; Heating;
参考文献
Dubbaka, Srinivas Reddy; Vogel, Pierre
Organic Letters, 2004 , vol. 6, # 1 p. 95 - 98
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in tetrahydrofuran; diethyl ether
30 h; Heating;
参考文献
Cho, Chul-Hee; Park, Heon; Park, Min-Ah; Ryoo, Tae-Yong; Lee, Yoon-Sik; Park, Kwangyong
European Journal of Organic Chemistry, 2005 , # 15 p. 3177 - 3181
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in tetrahydrofuran
28 h; Heating;
参考文献
Cho, Chul-Hee; Yun, Hee-Sung; Park, Kwangyong
Journal of Organic Chemistry, 2003 , vol. 68, # 8 p. 3017 - 3025
