Kostiner,E. et al.
Journal of Organometallic Chemistry, 1968 , vol. 15, p. 383 - 395
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Reddy et al.
Nature (London, United Kingdom), 1968 , vol. 217, p. 740
in further solvent(s)
byproducts: Ag; To soln. of Ag compd. in EtCN or PrCN twofold or stoich. amt. of elementadded, warmed at 21°C for <5 min; extd. with n-pentane, eluent evapd. in vac. at 0°C, purity checked by mass, (19)F and (13)C NMR spectra;
参考文献
Tyrra, Wieland; Wickleder, Mathias S.
Zeitschrift fur Anorganische und Allgemeine Chemie, 2002 , vol. 628, # 8 p. 1841 - 1847
in dimethyl sulfoxide
byproducts: (CH3)3SiF; HgF2 suspended in DMSO in a Schlenk-tube and (CH3)3SiC5F5 added to this soln. at room temp.; reacted for 48-72 h; solid precipitate filtered and washed with DMSO; filtrate and washing liquid added to water; precipitate collected by filtration and dried over concentrated H2SO4;
参考文献
Naumann, Dieter; Schulz, Frank
Zeitschrift fur Anorganische und Allgemeine Chemie, 2005 , vol. 631, # 1 p. 122 - 125
in pyridine
byproducts: CO2; refluxing under N2, 3h; evapn.; extn. (warm petrol); elem. anal.;
参考文献
Barassi, N. J.; Deacon, G. B.; Weigold, J. A.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1994 , vol. 620, p. 993 - 998
→
反应条件
in diethyl ether
参考文献
Miller, W. T.; Sun, K. K.
Journal of the American Chemical Society, 1970 , vol. 92, p. 6985 - 6987
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Gmelin Handbook: Ag: MVol.B5, 1.1.3, page 8 - 12
