6-氨基甲酰-2-吡啶羧酸合成路线 （共 5 条）
反应条件
trichlorophosphate 2 h; Heating / reflux;
参考文献
ALTANA PHARMA AG
Patent: WO2006/589 A1, 2006 ;
Location in patent: Page/Page column 57-58 ;
WO 2006/000589 A1
反应条件
ammonium hydroxide
T=90°C; 6 h;
参考文献
Veera Reddy; Jin; Arora; Sfeir; Feke Malon ey; Urbach; Sayre
Journal of the American Chemical Society, 1990 , vol. 112, # 6 p. 2332 - 2340
反应条件
1: 30 percent / concd. H2SO4 / H2O / 1.) reflux, 2 h, 2.) room temp.
2: 100 percent / concd. NH4OH / 6 h / 90 °C
View Scheme
参考文献
Veera Reddy; Jin; Arora; Sfeir; Feke Malon ey; Urbach; Sayre
Journal of the American Chemical Society, 1990 , vol. 112, # 6 p. 2332 - 2340
反应条件
hydrogenchloride; water
参考文献
Sato, Nagaaki; Jitsuoka, Makoto; Ishikawa, Shiho; Nagai, Keita; Tsuge, Hiroyasu; Ando, Makoto; Okamoto, Osamu; Iwaasa, Hisashi; Gomori, Akira; Ishihara, Akane; Kanatani, Akio; Fukami, Takehiro
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 6 p. 1670 - 1674
反应条件
ammonium hydroxide; dihydrogen peroxide
1.) H2O, 70 deg C, 3 h, 2.) 16 h; Yield given. Multistep reaction;
参考文献
Budzikiewicz, H.; Hildebrand, U.; Ockels, W.; Reiche, M.; Taraz, K.
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 4 p. 516 - 520
