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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
97522-31-1
合成路线
（共 10 条）
132959-46-7
→
反应条件
97522-31-1
反应条件
ammonium formate; palladium on activated charcoal in methanol T=25°C; 19 h;
参考文献
Burgess, Laurence E.; Meyers, A. I.
Journal of Organic Chemistry, 1992 , vol. 57, # 6 p. 1656 - 1662
97589-58-7
→
反应条件
97522-31-1
反应条件
potassium carbonate in methanol; water
参考文献
Nordlander, J. Eric; Njoroge, F. George; Payne, Mark J.; Warman, Dhiraj
Journal of Organic Chemistry, 1985 , vol. 50, # 19 p. 3481 - 3484
226991-18-0
(5S)-5-苄基-2-吡咯烷酮
→
反应条件
97522-31-1
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 4 h; Heating;
参考文献
Lebrun, Stephane; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre
Tetrahedron Asymmetry, 2003 , vol. 14, # 17 p. 2625 - 2632
132959-40-1
→
反应条件
97522-31-1
反应条件
1: 86 percent / LiAlH4 / diethyl ether; tetrahydrofuran / a) -78 deg C, 40 min, b) r.t., 15 h 2: 60 percent / HCOONH4 / 10percent Pd/C / methanol / 19 h / Ambient temperature View Scheme
参考文献
Burgess, Laurence E.; Meyers, A. I.
Journal of Organic Chemistry, 1992 , vol. 57, # 6 p. 1656 - 1662
958870-35-4
→
反应条件
97522-31-1
反应条件
ammonia; lithium T=-78°C; 0.5 h;
参考文献
Zeng, Wei; Chemler, Sherry R.
Journal of the American Chemical Society, 2007 , vol. 129, # 43 p. 12948 - 12949
36724-68-2
(S)-(-)-N-(三氟乙酰基)吡咯烷-2-羰酰氯
→
反应条件
97522-31-1
反应条件
1: 85 percent / AlCl3 / CH2Cl2 / 12 h / Ambient temperature 2: 85 percent / H2 / Pd/C / ethanol; diethyl ether 3: 65 percent / K2CO3 / methanol; H2O View Scheme
参考文献
Nordlander, J. Eric; Njoroge, F. George; Payne, Mark J.; Warman, Dhiraj
Journal of Organic Chemistry, 1985 , vol. 50, # 19 p. 3481 - 3484
97589-54-3
→
反应条件
97522-31-1
反应条件
1: 85 percent / H2 / Pd/C / ethanol; diethyl ether 2: 65 percent / K2CO3 / methanol; H2O View Scheme
参考文献
Nordlander, J. Eric; Njoroge, F. George; Payne, Mark J.; Warman, Dhiraj
Journal of Organic Chemistry, 1985 , vol. 50, # 19 p. 3481 - 3484
71-43-2
苯
→
反应条件
97522-31-1
反应条件
1: 85 percent / AlCl3 / CH2Cl2 / 12 h / Ambient temperature 2: 85 percent / H2 / Pd/C / ethanol; diethyl ether 3: 65 percent / K2CO3 / methanol; H2O View Scheme
参考文献
Nordlander, J. Eric; Njoroge, F. George; Payne, Mark J.; Warman, Dhiraj
Journal of Organic Chemistry, 1985 , vol. 50, # 19 p. 3481 - 3484
69311-30-4
→
反应条件
97522-31-1
+
63328-13-2
反应条件
L-leucinamide; streptavidin biotin-wild type; C42H64Cl4Ir2N6O4S2 in dimethyl sulfoxide T=30 - 50°C; pH=7.8; 18 h; Reagent/catalyst; Overall yield = 100 percent; enantioselective reaction;
参考文献
Quinto, Tommaso; Schwizer, Fabian; Zimbron, Jeremy M.; Morina, Albert; Koehler, Valentin; Ward, Thomas R.
ChemCatChem, 2014 , vol. 6, # 4 p. 1010 - 1014
606143-30-0
→
反应条件
97522-31-1
反应条件
1.1: trifluoroacetic acid / CH2Cl2 / 0.08 h / -78 °C 1.2: 90 percent / triethylsilane / CH2Cl2 / 13.5 h / -78 - 20 °C 2.1: magnesium monoperoxyphthalate / methanol / 20 °C 3.1: 85 percent / lithium aluminum hydride / tetrahydrofuran / 4 h / Heating View Scheme
参考文献
Lebrun, Stephane; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre
Tetrahedron Asymmetry, 2003 , vol. 14, # 17 p. 2625 - 2632
