反应条件
chlorine in dichloromethane
byproducts: ClC(NO2)2Me; dry Cl2 passed through soln. of the stibine in CH2Cl2 (30 min, 0°C), mixt. allowed to stand (20°C, 3 h); mixt. purged with dry N2; not isolated, GLC, TLC;
参考文献
Erashko, V. I.; Shevelev, S. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, p. 401 - 403
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , vol. 34, p. 439 - 442