2,4,6-三苯基环硼氮六烷合成路线 （共 17 条）
参考文献
Gmelin Handbook: B: B-Verb.9, 5.2.4, page 189 - 199
参考文献
Gmelin Handbook: B: B-Verb.9, 5.2.4, page 189 - 199
参考文献
Gmelin Handbook: B: B-Verb.9, 5.2.4, page 189 - 199
参考文献
Gmelin Handbook: B: B-Verb.9, 5.2.4, page 189 - 199
参考文献
Michailow; Kostroma
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1957 , p. 1125;engl.Ausg.S.1149,1150
反应条件
in toluene
byproducts: Me3SiCl, HCl; addn. of HN(SiMe3)2 to soln. of PhBCl2 (inert atmosphere), kept at 0°C for 30 min; warmed to ca 35°C, heated for 2 h at 120°C; cooling to room temp., volatiles removed (vac.), residue stirred overnight with hexane; insolubles collected, washed (hexane), dried (vac.): (BPhNH)3; filtrate concd., standing at room temp., ppt. collected, dried (vac.); elem. anal.;
参考文献
Niedenzu, Kurt; Serwatowska, Joanne; Serwatowski, Janusz
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1992 , vol. 47, # 5 p. 713 - 717
参考文献
Mikhailov, B. M.; Kostroma, T. V.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1957 , vol. 1957, p. 1125 - 1127
Full Text Show Details
Ruigh, W. L.; Gunderloy, F. C.; Sedlak, M.; Meulen, P. A. Van der
N.S.A., NP-5767 (1955) 1/35 1955 , vol. 9, p. 7267
