6-苄基氨基-1-(4’-苯基丁氧基)己烷合成路线 （共 9 条）
反应条件
triethylamine; sodium iodide
参考文献
Liu, Juntao; Zhou, Di; Jia, Xian; Huang, Ling; Li, Xingshu; Chan, Albert S.C.
Tetrahedron Asymmetry, 2008 , vol. 19, # 15 p. 1824 - 1828
反应条件
1: 51 percent / NaOH; tetra-n-butylammonium hydrogen sulphate; benzyltrimethylammonium chloride / CH2Cl2; H2O / 192 h / 20 °C 2: 38 percent / Cs2CO3 / dimethylformamide / 5 h / 60 - 80 °C View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 45, # 9 p. 755 - 762
反应条件
1: 51 percent / NaOH; tetra-n-butylammonium hydrogen sulphate; benzyltrimethylammonium chloride / CH2Cl2; H2O / 192 h / 20 °C 2: 38 percent / Cs2CO3 / dimethylformamide / 5 h / 60 - 80 °C View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 45, # 9 p. 755 - 762
反应条件
1: NaN3 / dimethylformamide 2: lithium aluminum hydride 3: 1.) mol. sieves; 2.) NaBH4 / 2.) ethanol View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 50 p. 9375 - 9378
反应条件
1: lithium aluminum hydride 2: 1.) mol. sieves; 2.) NaBH4 / 2.) ethanol View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 50 p. 9375 - 9378
反应条件
sodium tetrahydroborate; molecular sieve 2.) ethanol; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 35, # 50 p. 9375 - 9378
反应条件
1: 71 percent / acetonitrile / 1 h / Heating; other solvent 2: NaBH4 / methanol / 36 h / Ambient temperature 3: 0.21 g / H2 / Pd/C / methanol / 10 h View Scheme
参考文献
Rong, Yajing; Ruoho, Arnold E.
Synthetic Communications, 1999 , vol. 29, # 12 p. 2155 - 2162
反应条件
1: 71 percent / acetonitrile / 1 h / Heating; other solvent
2: NaBH4 / methanol / 36 h / Ambient temperature
View Scheme
参考文献
Rong, Yajing; Ruoho, Arnold E.
Synthetic Communications, 1999 , vol. 29, # 12 p. 2155 - 2162
反应条件
hydrogen; 5-palladium/activated carbon in ethanol
T=20°C; P=760.051 Torr;
参考文献
Bessa Bellmunt, Jordi; Dalmases Barjoan, Pere; Marquillas Olondriz, Francisco
Patent: US6388134 B1, 2002 ;
Location in patent: Page column 9 ;
