反应条件
1: 1.) NaH / 1.) THF, hexane, RT, 1 h, 2.) THF, hexane, reflux, 72 h
2: 90 percent / NaN3 / dimethylformamide / 6 h / 120 °C
3: 80 percent / LiAlH4 / tetrahydrofuran / 12 h / Ambient temperature
View Scheme
参考文献
Nangia, A.; Praveen, P.; Dubey, A. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 7 p. 629 - 631