三丁基(1-乙氧基乙烯)锡合成路线 （共 67 条）
反应条件
tributylphosphine in toluene toluene, 5 molpercent Ru-complex, tributylphosphine (30 mol percent) under 1 atm. ofH2, 80°C, 6 h;
参考文献
Shirakawa, Eiji; Morita, Ryotaro; Tsuchimoto, Teruhisa; Kawakami, Yusuke
Journal of the American Chemical Society, 2004 , vol. 126, # 42 p. 13614 - 13615
反应条件
1: With triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in toluene T=110°C; Stille coupling reaction; 24 h; 2: With hydrogenchloride in toluene T=20°C; 24 h;
参考文献
Legros, Jean-Yves; Primault, Gaelle; Fiaud, Jean-Claude
Tetrahedron, 2001 , vol. 57, # 13 p. 2507 - 2514
反应条件
1: With triphenylphosphine; lithium chloride; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane T=110°C; Stille coupling reaction; 24 h; 2: With hydrogenchloride in toluene T=20°C; 24 h;
参考文献
Legros, Jean-Yves; Primault, Gaelle; Fiaud, Jean-Claude
Tetrahedron, 2001 , vol. 57, # 13 p. 2507 - 2514
反应条件
1: With triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in toluene T=110°C; Stille coupling reaction; 1 h; 2: With hydrogenchloride in toluene T=20°C; 24 h;
参考文献
Legros, Jean-Yves; Primault, Gaelle; Fiaud, Jean-Claude
Tetrahedron, 2001 , vol. 57, # 13 p. 2507 - 2514
反应条件
benzoylchlorobis(triphenylphosphine)palladium(II) in toluene T=110°C; 3 h; other catalyst: (CH3CN)2Cl2Pd;
参考文献
Clerici, Francesca; Erba, Emanuela; Gelmi, Maria Luisa; Valle, Marinella
Tetrahedron, 1997 , vol. 53, # 46 p. 15859 - 15866
反应条件
1: With triphenylphosphine; lithium chloride; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane T=110°C; Stille coupling reaction; 24 h; 2: With hydrogenchloride in toluene T=20°C; 24 h;
参考文献
Legros, Jean-Yves; Primault, Gaelle; Fiaud, Jean-Claude
Tetrahedron, 2001 , vol. 57, # 13 p. 2507 - 2514
反应条件
1: With triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in toluene T=110°C; Stille coupling reaction; 24 h; 2: With hydrogenchloride in toluene T=20°C; 24 h;
参考文献
Legros, Jean-Yves; Primault, Gaelle; Fiaud, Jean-Claude
Tetrahedron, 2001 , vol. 57, # 13 p. 2507 - 2514
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=100°C; 18 h; Inert atmosphereSealed tube; 2: With hydrogenchloride in 1,4-dioxane; methanol
参考文献
MERCK SHARP andamp;; DOHME CORP.; ALTMAN, Michael, D.; BILODEAU, Mark, T.; LIM, Jongwon; NORTHRUP, Alan; STANTON, Matthew, G.; TAOKA, Brandon, M.
Patent: WO2010/83145 A1, 2010 ;
Location in patent: Page/Page column 56-57 ;
WO 2010/083145 A1
反应条件
hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride in toluene T=100°C; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 2 p. 767 - 768
反应条件
hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride in toluene T=100°C; 20 h;
参考文献
Kosugi, Masanori; Sumiya, Takashi; Obara, Yukimasa; Suzuki, Motohiro; Sano, Hiroshi; Migita, Toshihiko
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 767 - 768
