三丁基(1-乙氧基乙烯)锡合成路线 (共 67 条)
反应条件
hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride in toluene T=100°C; 20 h;
参考文献
Kosugi, Masanori; Sumiya, Takashi; Obara, Yukimasa; Suzuki, Motohiro; Sano, Hiroshi; Migita, Toshihiko
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 767 - 768
参考文献
Angewandte Chemie - International Edition, , vol. 39, # 9 p. 1629 - 1632
反应条件
hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride in toluene T=80°C; 20 h;
参考文献
Kosugi, Masanori; Sumiya, Takashi; Obara, Yukimasa; Suzuki, Motohiro; Sano, Hiroshi; Migita, Toshihiko
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 767 - 768
反应条件
hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride in toluene T=80°C; 20 h;
参考文献
Kosugi, Masanori; Sumiya, Takashi; Obara, Yukimasa; Suzuki, Motohiro; Sano, Hiroshi; Migita, Toshihiko
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 767 - 768
反应条件
hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride in benzene T=100°C; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 2 p. 767 - 768
反应条件
hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride in toluene T=80°C; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 2 p. 767 - 768
参考文献
Song, Yonghong; Clizbe, Lane; Bhakta, Chhaya; Teng, Willy; Li, Wenhao; Wong, Paul; Huang, Brian; Sinha, Uma; Park, Gary; Reed, Andrea; Scarborough, Robert M; Zhu, Bing-Yan
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 15 p. 2043 - 2046
反应条件
1: With tetrakis(triphenylphosphine) palladium(0) in toluene T=105 - 112°C; 48 h; Inert atmosphere; 2: With hydrogenchloride in tetrahydrofuran T=20°C; 3: With sodium hydrogencarbonate in tetrahydrofuran pH=8;
参考文献
VARINEL INC; ZURAWSKI JR, Vincent R.; STOUT, David M.; NITZ, Theodore J.
Patent: WO2012/20389 A1, 2012 ;
Location in patent: Page/Page column 34-35 ;
WO 2012/020389 A1
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=100°C; Stille coupling;
参考文献
Givens, Richard S.; Stensrud, Kenneth; Conrad, Peter G.; Yousef, Abraham L.; Perera, Chamani; Senadheera, Sanjeewa N.; Heger, Dominik; Wirz, Jakob
Canadian Journal of Chemistry, 2011 , vol. 89, # 3 p. 364 - 384
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=150°C; 0.5 h; Microwave irradiation;
参考文献
IRM LLC; NOVARTIS AG; CHIANELLI, Donatella; LI, Xiaolin; LIU, Xiaodong; LOREN, Jon; MOLTENI, Valentina; NABAKKA, Juliet; REVESZ, Laszlo; PEREZ, Lawrence B.; BROOKS, Clinton; WRONA, Wojciech; MANLEY, Paul W.; BREITENSTEIN, Werner
Patent: WO2008/58037 A1, 2008 ;
Location in patent: Page/Page column 32 ;
WO 2008/058037 A1