三丁基(1-乙氧基乙烯)锡合成路线 （共 67 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
4 h; Heating / reflux;
参考文献
Chu, Shao Song; Alegria, Larry Andrew; Bleckman, Ted Michael; Chong, Wesley Kwan Mung; Duvadie, Rohit K.; Li, Lin; Reich, Siegfried Heinz; Romines III, William Henry; Wallace, Michael B.; Yang, Yi
Patent: US2003/225147 A1, 2003 ;
Location in patent: Page 35 ;
反应条件
1: With triphenylphosphine; lithium chloride; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane
T=110°C; Stille coupling reaction; 24 h;
2: With hydrogenchloride in toluene
T=20°C; 24 h;
参考文献
Legros, Jean-Yves; Primault, Gaelle; Fiaud, Jean-Claude
Tetrahedron, 2001 , vol. 57, # 13 p. 2507 - 2514
反应条件
bis-triphenylphosphine-palladium(II) chloride in 1,4-dioxane
T=90°C; 2 h;
参考文献
Iwanowicz, Edwin J.; Watterson, Scott H.; Guo, Junqing; Pitts, William J.; Murali Dhar; Shen, Zhongqi; Chen, Ping; Gu, Henry H.; Fleener, Catherine A.; Rouleau, Katherine A.; Cheney, Daniel L.; Townsend, Robert M.; Hollenbaugh, Diane L.
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 12 p. 2059 - 2063
反应条件
copper(l) iodide; triphenyl-arsane; tris-(dibenzylideneacetone)dipalladium(0) in N,N-dimethyl-formamide
T=60°C; 6 h;
参考文献
Farina, Vittorio; Kapadia, Suresh; Krishnan, Bala; Wang, Chenjie; Liebeskind, Lanny S.
Journal of Organic Chemistry, 1994 , vol. 59, # 20 p. 5905 - 5911
反应条件
tert.-butyl lithium in hexane
T=0°C; 5 h;
参考文献
Sorger, Klas; Bauer, Walter; Schleyer, Paul von Rague; Stalke, Dietmar
Angewandte Chemie, 1995 , vol. 107, # 15 p. 1766 - 1768
反应条件
bis(triphenylphosphine)palladium(II)-chloride in N,N-dimethyl-formamide
T=60°C; 8 h;
参考文献
Dalton, Audra M.; Zhang, Yongjun; Davie, Christopher P.; Danheiser, Rick L.
Organic Letters, 2002 , vol. 4, # 15 p. 2465 - 2468
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
T=160°C; 0.25 h; Microwave irradiation;
2: With hydrogenchloride; water in N,N-dimethyl-formamide
T=20°C; 1 h;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GmbH; CARSON, Rebekah J.; FADER, Lee; KAWAI, Stephen; LANDRY, Serge
Patent: WO2009/62288 A1, 2009 ;
Location in patent: Page/Page column 67-68 ;
