2,6-二氯烟酸甲酯 N-氧化物合成路线 （共 4 条）
反应条件
1: 1.) 5 eq.Na / 2.) room t., 6 h 2: 86 percent / 2 M HCl / methanol / 0.25 h / Heating 3: 2 M NaOH / methanol / 0.5 h / Heating View Scheme
参考文献
Dainter, Ronald S.; Suschitzky, Hans; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 227 - 234
反应条件
1: 1.) 5 eq.Na / 2.) room t., 6 h 2: 86 percent / 2 M HCl / methanol / 0.25 h / Heating View Scheme
参考文献
Dainter, Ronald S.; Suschitzky, Hans; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 227 - 234
反应条件
1: 1.) 5 eq.Na / 2.) room t., 6 h 2: 86 percent / 2 M HCl / methanol / 0.25 h / Heating 3: 84 percent / H2 / 5 percent Pd/C / methanol / Ambient temperature; in presence of KOAc 4: 2 M NaOH / methanol / 0.5 h / Heating View Scheme
参考文献
Dainter, Ronald S.; Suschitzky, Hans; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 227 - 234
反应条件
1: 1.) 5 eq.Na / 2.) room t., 6 h 2: 86 percent / 2 M HCl / methanol / 0.25 h / Heating 3: 84 percent / H2 / 5 percent Pd/C / methanol / Ambient temperature; in presence of KOAc View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 227 - 234
