1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / |Inert atmosphere 1.2: 1 h / -78 °C / |Inert atmosphere 2.1: pyridinium chlorochromate / dichloromethane / 20 °C View Scheme
参考文献
Chu, Ling; Wang, Xiao-Chen; Moore, Curtis E.; Rheingold, Arnold L.; Yu, Jin-Quan
Journal of the American Chemical Society, 2013 , vol. 135, # 44 p. 16344 - 16347
N,N,N-trimethylbenzenemethanaminium dichloroiodate; zinc(II) chloride in acetic acid T=70°C; 24 h; with prereaction of the reagents; Product distribution;
aluminium trichloride; chlorine in tetrachloromethane; chloroform T=0 - 20°C; 14 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Raggon, Jeffrey W.; Welborn, Jennifer M.; Godlewski, Jane E.; Kelly, Sarah E.; LaCour, Thomas G.
Organic Preparations and Procedures International, 1995 , vol. 27, # 2 p. 233 - 236