反应条件
1.1: [Cu(I)(CH3CN)4]PF6; (S,S)-Ph-BPE; Li(OC6H4-p-OMe) / tetrahydrofuran; N,N-dimethyl-formamide / 48 h / -70 °C / Inert atmosphere 1.2: 40 h / -78 - 20 °C 2.1: tetrakis(triphenylphosphine) palladium(0); N,N'-dimethyl-barbituric acid / dichloromethane / 6 h / 50 °C 3.1: potassium carbonate / dichloromethane; water / 2.5 h / 20 °C 4.1: lithium aluminium tetrahydride / tetrahydrofuran / 48 h / Reflux 5.1: sodium hydride / dimethyl sulfoxide; mineral oil / 1 h / 20 °C 5.2: 1 h / 50 °C View Scheme
参考文献
Suzuki, Yuta; Iwata, Mitsutaka; Yazaki, Ryo; Kumagai, Naoya; Shibasaki, Masakatsu
Journal of Organic Chemistry, 2012 , vol. 77, # 9 p. 4496 - 4500
