in methanol
Sn-complex and ligand were stirred in MeOH at room temp. for ca. 12 h; filtered, washed with EtOH, dried under vac. at 20°C for 10 h; elem. anal.;
参考文献
Cunningham, Desmond; Firtear, Padraig; Molloy, Kiaran C.; Zuckerman, Jerald J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 1523 - 1528
in methanol
Sn-complex and ligand were stirred in MeOH at room temp. for ca. 12 h; filtered, washed with EtOH, dried under vac. at 20°C for 10 h; elem. anal.;
参考文献
Cunningham, Desmond; Firtear, Padraig; Molloy, Kiaran C.; Zuckerman, Jerald J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 1523 - 1528
in water
soln. of Sn-complex in H2O was added to soln. of ligand in H2O at room temp.; filtered, washed with EtOH, dried under vac. at 20°C for 10 h; elem. anal.;
参考文献
Cunningham, Desmond; Firtear, Padraig; Molloy, Kiaran C.; Zuckerman, Jerald J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 1523 - 1528
Palmer; Scott
Journal of the American Chemical Society, 1928 , vol. 50, p. 541
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Binz; Bauer; Hallstein
Chemische Berichte, 1920 , vol. 53, p. 427
