3-chloroprop-1-ene in ethylene glycol dimethyl ether under argon; tin compound in DME cooled to -78 °C; nBuLi added; quench with excess alkyl halide;; poured in NH4Cl-soln./petroleum ether; sepn. of org. layer; dried; concd.; chromd.; NMR;
参考文献
Journal of the American Chemical Society, , vol. 110, p. 842