hydrogen; 2C2H3O2(1-)*4C8H12*2Rh(1+); C54H60O6P2 in toluene T=20 - 60°C; P=3750.38 Torr; 17 h; Conversion of starting material;
参考文献
MITSUBISHI CHEMICAL CORPORATION; THE RESEARCH FOUNDATION OF STATE UNIVERSITY OF NEW YORK
Patent: WO2004/76464 A2, 2004 ;
Location in patent: Page/Page column 70 ;
RhH2(O2COH)(P(i-Pr)3)2 in tetrahydrofuran T=120°C; 20 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
