RhH2(O2COH)(P(i-Pr)3)2 in tetrahydrofuran T=120°C; 20 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
RhH2(O2COH)(P(i-Pr)3)2 in tetrahydrofuran T=120°C; 20 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
RhH2(O2COH)(P(i-Pr)3)2 in tetrahydrofuran T=120°C; 20 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
Wyrick, Steven D.; Booth, Raymond G.; Myers, Andrew M.; Owens, Constance E.; Bucholtz, Ehren C.; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 19 p. 3857 - 3864
1: With ammonium metavanadate; tetrabutylammomium bromide; toluene-4-sulfonic acid in water; acetonitrile T=20°C; 12 h; 2: With silica gel in hexane; ethyl acetate Column chromatography;
参考文献
Kikushima, Kotaro; Moriuchi, Toshiyuki; Hirao, Toshikazu
Chemistry - An Asian Journal, 2009 , vol. 4, # 8 p. 1213 - 1216