boron trifluoride diethyl etherate in dichloromethane
T=0°C; 0.333333 h;
参考文献
Miura, Masahiro; Yoshida, Masaya; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Chemical Communications, 1982 , # 7 p. 397 - 398
Miura, Masahiro; Yoshida, Masaya; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Chemical Communications, 1982 , # 7 p. 397 - 398
in dichloromethane
under N2, freshly distd. 2-phenylpropene added dropwise to CH2Cl2 soln.of BHBr2*SMe2 with water bath (15°C), cooled, mixt. left overnight at room temp., 1,3-bis(trimethylsiloxy)propane added, stirred for 3 h; solvent and volatiles removed by aspirator vac.;
参考文献
Brown; Imai
Journal of the American Chemical Society, 1983 , vol. 105, # 20 p. 6285 - 6289