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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
α-甲基苯乙烯
合成路线
（共 1062 条）
98-83-9
α-甲基苯乙烯
→
反应条件
58617-67-7
反应条件
N-iodo-succinimide; n-Bu4NH2F3 in dichloromethane T=0°C; 1 h; other fluorid ion source, other solvents, other rection times, other temperature, 1,3-dibromo-5,5-dimethylhydantoin for bromofluorination;
参考文献
Kuroboshi, Manabu; Hiyama, Tamejiro
Tetrahedron Letters, 1991 , vol. 32, # 9 p. 1215 - 1218
98-83-9
α-甲基苯乙烯
→
反应条件
60212-12-6
+
58617-67-7
反应条件
N-iodo-succinimide; KHF2; hydrogen fluoride; tetrabutyl ammonium fluoride in dichloromethane T=0 - 20°C; 9 h;
参考文献
Kuroboshi, Manabu; Hiyama, Tamejiro
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 7 p. 1799 - 1806
98-83-9
α-甲基苯乙烯
→
反应条件
59647-78-8
2-苯基丙醛肟
反应条件
1: nitric acid / 0.33 h / 0 °C 2: triethylamine / chloroform / 3 h / 20 °C 3: glucose dehydrogenase; pentaerythritol tetranitrate reductase from Enterobacter cloacae PB2; D-glucose; nicotinamide adenine dinucleotide / 24 h / 30 °C / pH 7.5 / aq. buffer; Enzymatic reaction View Scheme
参考文献
Durchschein, Katharina; Fabian, Walter M. F.; MacHeroux, Peter; Zangger, Klaus; Trimmel, Gregor; Faber, Kurt
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3364 - 3369
98-83-9
α-甲基苯乙烯
→
反应条件
59647-78-8
2-苯基丙醛肟
反应条件
1: nitric acid / 0.33 h / 0 °C 2: triethylamine / chloroform / 3 h / 20 °C 3: glucose dehydrogenase; xenobiotic reductase A from Pseudomonas putida; D-glucose; NADP / 24 h / 30 °C / pH 7.5 / aq. buffer; Enzymatic reaction View Scheme
参考文献
Durchschein, Katharina; Fabian, Walter M. F.; MacHeroux, Peter; Zangger, Klaus; Trimmel, Gregor; Faber, Kurt
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3364 - 3369
98-83-9
α-甲基苯乙烯
→
反应条件
59647-78-8
2-苯基丙醛肟
反应条件
1: nitric acid / 0.33 h / 0 °C 2: triethylamine / chloroform / 3 h / 20 °C 3: xenobiotic reductase B from Pseudomonas putida JLR11; Reduced nicotinamide-adenine dinucleotide / 24 h / 30 °C / pH 7.5 / aq. buffer; Enzymatic reaction View Scheme
参考文献
Durchschein, Katharina; Fabian, Walter M. F.; MacHeroux, Peter; Zangger, Klaus; Trimmel, Gregor; Faber, Kurt
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3364 - 3369
98-83-9
α-甲基苯乙烯
→
反应条件
59888-14-1
反应条件
pyridine hydrogenfluoride; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile Ambient temperature;
参考文献
Lal, G. Sankar
Journal of Organic Chemistry, 1993 , vol. 58, # 10 p. 2791 - 2796
98-83-9
α-甲基苯乙烯
→
反应条件
59974-27-5
(1-溴-2-氟-2-丙基)苯
反应条件
N-bromosuccinmide; Me3N*2HF in dichloromethane T=0 - 20°C; Addition; fluorination; bromination;
参考文献
Oldendorf, Jens; Haufe, Guenter
Advanced Synthesis and Catalysis, 2000 , vol. 342, # 1 p. 52 - 57
98-83-9
α-甲基苯乙烯
→
反应条件
59974-27-5
(1-溴-2-氟-2-丙基)苯
+
36043-44-4
+
3360-54-1
(1-溴甲基-乙烯基)-苯
反应条件
N-bromosuccinmide; n-Bu4NH2F3 in dichloromethane 1 h; Heating;
参考文献
Albanese, Domenico; Landini, Dario; Penso, Michele; Pratelli, Marco
Gazzetta Chimica Italiana, 1991 , vol. 121, # 12 p. 537 - 541
→
反应条件
6006-81-1
beta-亚甲基苯乙醇
反应条件
selenium(IV) oxide; acetic acid in decane; dichloromethane
参考文献
Wako Pure Chemical Industies, Ltd.; JAPAN SCIENCE AND TECHNOLOGY CORPORATION
Patent: EP1537913 A1, 2005 ;
98-83-9
α-甲基苯乙烯
→
反应条件
6006-81-1
beta-亚甲基苯乙醇
反应条件
tert.-butylhydroperoxide; selenium(IV) oxide; 2,2,4-trimethylpentane in dichloromethane 4 h; Ambient temperature;
参考文献
Gazzard, Lewis J.; Motherwell, William B.; Sandham, David A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 979 - 993
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