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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
DL-1-苯乙醇
合成路线
（共 1445 条）
406-95-1
2,2,2-三氟乙酸乙酯
+
98-85-1
DL-1-苯乙醇
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
16197-92-5
反应条件
Burkholderia cepacia lipase; C13H24N3(1+)*C36H73O14S(1-) in di-isopropyl ether T=35°C; 0.5 h; Kinetics; Reagent/catalystTime; optical yield given as percent eeenantioselective reaction;
参考文献
Abe, Yoshikazu; Hirakawa, Takuya; Nakajima, Shino; Okano, Nagisa; Hayase, Shuichi; Kawatsura, Motoi; Hirose, Yoshihiko; Itoh, Toshiyuki
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 13 p. 1954 - 1958
98-85-1
DL-1-苯乙醇
+
802294-64-0
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
107832-32-6
+
120-45-6
丙酸苏合香酯
反应条件
Birman's catalyst; trimethylacetic anhydride; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 12 h; optical yield given as percent eeenantioselective reaction;
参考文献
Shiina, Isamu; Nakata, Kenya; Sugimoto, Masuhiro; Onda, Yu-Suke; Iizumi, Takashi; Ono, Keisuke
Heterocycles, 2009 , vol. 77, # 2 p. 801 - 810
98-85-1
DL-1-苯乙醇
+
501-52-0
3-苯基丙酸
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
52126-27-9
+
52126-26-8
反应条件
Birman's catalyst; trimethylacetic anhydride; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 12 h; optical yield given as percent eeenantioselective reaction;
参考文献
Shiina, Isamu; Nakata, Kenya; Sugimoto, Masuhiro; Onda, Yu-Suke; Iizumi, Takashi; Ono, Keisuke
Heterocycles, 2009 , vol. 77, # 2 p. 801 - 810
98-85-1
DL-1-苯乙醇
+
66-77-3
1-萘甲醛
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
反应条件
(5aS,10bR)-5a,10b-dihydro-2-(pentafluorophenyl)-4H,6H-indeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazinium tetrafluoroborate; 3-benzylriboflavin tetraacetate; triethylamine in toluene T=20°C; 19 h; Resolution of racemateAirMolecular sieve; optical yield given as percent eeenantioselective reaction;
参考文献
Iwahana, Soichiro; Iida, Hiroki; Yashima, Eiji
Chemistry - A European Journal, 2011 , vol. 17, # 29 p. 8009 - 8013
98-85-1
DL-1-苯乙醇
+
100-52-7
苯甲醛
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
13358-49-1
反应条件
(5aS,10bR)-5a,10b-dihydro-2-(pentafluorophenyl)-4H,6H-indeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazinium tetrafluoroborate; 3-benzylriboflavin tetraacetate; triethylamine in toluene T=20°C; 4 h; Resolution of racemateAirMolecular sieve; optical yield given as percent eeenantioselective reaction;
参考文献
Iwahana, Soichiro; Iida, Hiroki; Yashima, Eiji
Chemistry - A European Journal, 2011 , vol. 17, # 29 p. 8009 - 8013
98-85-1
DL-1-苯乙醇
+
66-99-9
2-萘甲醛
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
74764-98-0
反应条件
(5aS,10bR)-5a,10b-dihydro-2-(pentafluorophenyl)-4H,6H-indeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazinium tetrafluoroborate; 3-benzylriboflavin tetraacetate; triethylamine in toluene T=20°C; 19 h; Resolution of racemateAirMolecular sieve; optical yield given as percent eeenantioselective reaction;
参考文献
Iwahana, Soichiro; Iida, Hiroki; Yashima, Eiji
Chemistry - A European Journal, 2011 , vol. 17, # 29 p. 8009 - 8013
98-85-1
DL-1-苯乙醇
+
123-62-6
丙酸酐
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
120-45-6
丙酸苏合香酯
反应条件
(-)-Tetramisole; N-ethyl-N,N-diisopropylamine in chloroform T=0°C; 13 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Klauck, Maggie I.; Patel, Sachin G.; Wiskur, Sheryl L.
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3570 - 3575
84782-03-6
+
98-85-1
DL-1-苯乙醇
→
反应条件
5978-70-1
+
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
116907-37-0
+
149403-13-4
+
107832-32-6
反应条件
lipase B from Candida antarctica in toluene T=78°C; 48 h; Enzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
133-89-1
+
98-85-1
DL-1-苯乙醇
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
74284-26-7
反应条件
HEPES buffer; Nicotiana tabacum GTF-II glucosyltransferase T=35°C; pH=7.0; 36 h; Enzymatic reaction;
参考文献
Shimoda, Kei; Kubota, Naoji; Hamada, Hiroki
Tetrahedron Asymmetry, 2004 , vol. 15, # 15 p. 2319 - 2321
5809-91-6
+
98-85-1
DL-1-苯乙醇
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
763132-65-6
反应条件
CAL B T=35°C; 0.5 h; Resolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Lourenco, Nuno M. T.; Monteiro, Carlos M.; Afonso, Carlos A. M.
European Journal of Organic Chemistry, 2010 , # 36 p. 6938 - 6943
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