pyridine; tetrabutylammomium bromide; copper(I) bromide in N,N-dimethyl-formamide T=-10 - -5°C; Electrochemical reaction; Title compound not separated from byproducts;
T=180°C; 17 h; other reaction time, reagent ratio; Product distribution;
参考文献
Gazizov, M. B.; Kachalova, T. N.; Karimova, R. F.; Khairullin, R. A.; Sinyashin, O. G.
Russian Journal of General Chemistry, 1997 , vol. 67, # 12 p. 1942 - 1943
Zhurnal Obshchei Khimii, 1997 , vol. 67, # 12 p. 2055 - 2056
T=180°C; 17 h; other gem-dihalide: benzal bromide, other methyl esters of tetracoordinated phosphorus acids, various reactants ratio, other reaction temperature and time; Product distributionMechanism;
Al(III) salt; tetrabutylammomium bromide in N,N-dimethyl-formamide P=18240 Torr; anode = Al 99.9percent ; cathode = Zn 99percent ; cathodic current density 100 A m-2;
