2-氯-5-甲氧基-4-肼基嘧啶合成路线 (共 4 条)
反应条件
bromocyane; sodium methylate in methanol; acetonitrile; tert-butyl alcohol T=0 - 41°C; 7 h;
参考文献
Dow AgroSciences LLC
Patent: US6362335 B1, 2002 ;
Location in patent: Page column 7 ;
反应条件
sodium methylate in acetonitrile; tert-butyl alcohol T=21 - 42°C; 5.2 h;
参考文献
Dow AgroSciences LLC
Patent: US6362335 B1, 2002 ;
Location in patent: Example 8 ;
反应条件
sodium carbonate in methanol; water; toluene
参考文献
Emonds, Mark Victor Michael; Roth, Gary A.
Patent: US2002/13230 A1, 2002 ;
反应条件
sodium carbonate; hydrazine in methanol; water; toluene
T=15 - 42°C; 4.1 h;
参考文献
Dow AgroSciences LLC
Patent: US6362335 B1, 2002 ;
Location in patent: Example 2-3 ;