反应条件
1: phenyllithium With copper (I) cyanide in tetrahydrofuran; diethyl ether; hexane
T=-30 - -10°C; 0.166667 h; Inert atmosphere;
2: 1-chloro-1-methyl-2-(hydroxyimino)ethane in tetrahydrofuran; diethyl ether; hexane
T=-30°C; 0.333333 h; Inert atmosphere;
3: With sulfuric acid in tetrahydrofuran; diethyl ether; hexane; dichloromethane
T=-30°C; Inert atmosphere;
参考文献
Sengupta, Ritobroto; Weinreb, Steven M.
Synthesis (Germany), 2012 , vol. 44, # 18 p. 2933 - 2937