1-乙酰基-4-碘-1H-吡唑合成路线 (共 2 条)
反应条件
triethylamine in dichloromethane T=0 - 20°C;
参考文献
Jacques, Vincent; Rusche, James R.; Peet, Norton P.; Singh, Jasbir
Patent: US2013/317003 A1, 2013 ;
Location in patent: Paragraph 0479 ;
反应条件
palladium diacetate; triethylamine; phosphorous acid trimethyl ester in N,N-dimethyl-formamide
T=80°C; Heck Reaction; 1 h; Inert atmosphere;
参考文献
Kwok, Thomas J.; Virgilio, Joseph A.
Organic Process Research and Development, 2005 , vol. 9, # 5 p. 694 - 696