2,5-二(5-溴噻吩-2-基)噻吩合成路线 （共 7 条）
反应条件
N-bromosuccinmide in chloroform; acetic acid RT, 1 h; 50-60 deg C, 30 min;
参考文献
Yui, Koji; Aso, Yoshio; Otsubo, Tetsuo; Ogura, Fumio
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 5 p. 1539 - 1546
反应条件
N-bromosuccinmide; acetic acid in chloroform Ambient temperature;
参考文献
Nakayama, Juzo; Konishi, Toru; Murabayashi, Shigeru; Hoshino, Masamatsu
Heterocycles, 1987 , vol. 26, # 7 p. 1793 - 1796
反应条件
N-bromosuccinmide in tetrachloromethane 48 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 44, # 9 p. 2403 - 2412
反应条件
anhydrous iron chloride; 2-bromo-3,4-dichloropyridazin-3(2H)-one in dichloromethane T=20°C; 0.166667 h; regioselective reaction;
参考文献
Bulletin of the Korean Chemical Society, , vol. 31, # 10 p. 2985 - 2988
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; potassium hydroxide; aluminum oxide T=70°C; Suzuki coupling; 0.183333 h; microwave irradiation;
参考文献
Melucci, Manuela; Barbarella, Giovanna; Sotgiu, Giovanna
Journal of Organic Chemistry, 2002 , vol. 67, # 25 p. 8877 - 8884
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in diethyl ether 0.5 h; Heating;
参考文献
Pham, Chiem Van; Burkhardt, A.; Shabana, R.; Cunningham, David D.; Mark, Harry B.; Zimmer, Hans
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 46, p. 153 - 168
反应条件
1: thien-2-yl bromide With magnesium in tetrahydrofuran T=20°C; Reflux; 2: 5,5''-dibromo-[2,2':5',2'']-terthiophene With [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran Grignard reaction;
参考文献
Jiang, Chuanyu; Liu, Ping; Deng, Wenji
Synthetic Communications, 2009 , vol. 39, # 13 p. 2360 - 2369
