1: 80 percent / NaH / 1.5 h / 80 °C 2: Ac2O / 2 h / 130 °C 3: CH2Cl2 / 0.5 h / Ambient temperature 4: NaH / 1,2-dimethoxy-ethane / 3 h / 80 °C 5: aq. NaOH / tetrahydrofuran / 1.5 h / 80 °C 6: 21.3 g / various solvent(s) / 24 h / 110 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 28, # 11 p. 1558 - 1564
1: Ac2O / 2 h / 130 °C 2: CH2Cl2 / 0.5 h / Ambient temperature 3: NaH / 1,2-dimethoxy-ethane / 3 h / 80 °C 4: aq. NaOH / tetrahydrofuran / 1.5 h / 80 °C 5: 21.3 g / various solvent(s) / 24 h / 110 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 28, # 11 p. 1558 - 1564
1: CH2Cl2 / 0.5 h / Ambient temperature 2: NaH / 1,2-dimethoxy-ethane / 3 h / 80 °C 3: aq. NaOH / tetrahydrofuran / 1.5 h / 80 °C 4: 21.3 g / various solvent(s) / 24 h / 110 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 28, # 11 p. 1558 - 1564
