dihydrogen peroxide in acetic acid 94 h; Ambient temperature;

1: 80 percent 2: 1.) sodium hydride / 1.) DMF, mineral oil, 30 min, r.t.; 2.) 5 h, 50 deg C 3: 90 percent / 36percent H2O2 / acetic acid / 94 h / Ambient temperature View Scheme

1: 80 percent 2: 1.) sodium hydride / 1.) DMF, mineral oil, 30 min, r.t.; 2.) 5 h, 50 deg C 3: 90 percent / 36percent H2O2 / acetic acid / 94 h / Ambient temperature View Scheme

1: 1.) sodium hydride / 1.) DMF, mineral oil, 30 min, r.t.; 2.) 5 h, 50 deg C 2: 90 percent / 36percent H2O2 / acetic acid / 94 h / Ambient temperature View Scheme