3,4-二氢-2H-噻喃-5-羧酸1-氧化物合成路线 (共 5 条)
反应条件
MPPA; diethyl ether
T=-40°C;
参考文献
Korte; Loehmer
Chemische Berichte, 1958 , vol. 91, p. 1397,1403
反应条件
1: magnesium bromide-diisopropylamide; diethyl ether
2: hydrogen chloride
3: aqueous KOH-solution
4: monoperoxyphthalic acid; diethyl ether / -40 °C
View Scheme
参考文献
Korte; Loehmer
Chemische Berichte, 1958 , vol. 91, p. 1397,1403
反应条件
1: aqueous KOH-solution
2: monoperoxyphthalic acid; diethyl ether / -40 °C
View Scheme
参考文献
Korte; Loehmer
Chemische Berichte, 1958 , vol. 91, p. 1397,1403
反应条件
1: hydrogen chloride
2: aqueous KOH-solution
3: monoperoxyphthalic acid; diethyl ether / -40 °C
View Scheme
参考文献
Korte; Loehmer
Chemische Berichte, 1958 , vol. 91, p. 1397,1403
反应条件
1: 260 °C
2: magnesium bromide-diisopropylamide; diethyl ether
3: hydrogen chloride
4: aqueous KOH-solution
5: monoperoxyphthalic acid; diethyl ether / -40 °C
View Scheme
参考文献
Korte; Loehmer
Chemische Berichte, 1958 , vol. 91, p. 1397,1403