1-(2,4-二溴苯基)-2-(1H-1,2,4-噻唑-1-基)-乙酮合成路线 （共 3 条）
反应条件
sulfuric acid; sodium nitrite in water
T=0 - 20°C; 2 h;
参考文献
Krimer, M. Z.; Tashi, B. P.; Roitburd, G. V.; Shtirkov, I. M.; Manaev, S. A.; et al.
Doklady Chemistry, 1989 , vol. 308, # 4-6 p. 299 - 301
Dokl. Akad. Nauk SSSR Ser. Khim., 1989 , vol. 308, # 5 p. 1155 - 1158
反应条件
1: acetonitrile / 80 - 85 °C
2: conc. H2SO4, NaNO2 / H2O / 2 h / 0 - 20 °C
View Scheme
参考文献
Krimer, M. Z.; Tashi, B. P.; Roitburd, G. V.; Shtirkov, I. M.; Manaev, S. A.; et al.
Doklady Chemistry, 1989 , vol. 308, # 4-6 p. 299 - 301
Dokl. Akad. Nauk SSSR Ser. Khim., 1989 , vol. 308, # 5 p. 1155 - 1158
反应条件
sulfuric acid; sodium nitrite in water; acetonitrile
T=20°C; 20 h; other 4-amino-1-phenacyl-1,2,4-triazolium bromides; Product distributionMechanism;
参考文献
Shtyrkov, I. M.; Roitburd, G. V.; Tashchi, V. P.; Krimer, M. Z.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 12 p. 2460 - 2463
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , vol. 40, # 12 p. 2821 - 2824
