暂无反应条件数据

暂无反应条件数据

Stage #1: <b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '110354', constants.ctx, '0')">4-(N,N-dimethlyamino)pyridine</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '8189822', constants.ctx, '0')">Wang resin</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '878281', constants.ctx, '0')">diisopropyl-carbodiimide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />T=0 - 20&deg;C;&nbsp;Solid phase reaction;&nbsp;esterification;&nbsp;18&nbsp;h;&nbsp;<br />Stage #2: <b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11460447', constants.ctx, '0')">lithium aluminium tetrahydride</a> <br />Solid phase reaction;&nbsp;reduction;&nbsp;&nbsp;Further stages.;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11343078', constants.ctx, '0')">sodium tetrahydroborate</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1098229', constants.ctx, '0')">methanol</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />2.5&nbsp;h;&nbsp;&nbsp;Ambient temperature;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: 0.70 g / Rh(OAc)4 / CH₂Cl₂ / 0.5 h / 20 &deg;C<br />2: LiAlH₄ / diethyl ether / 0.5 h / -60 - -30 &deg;C<br />3: 55 mg / aq. H₂O₂; KF; KHCO₃ / diethyl ether; methanol / 15 h / 20 &deg;C<br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '2349612', constants.ctx, '0')">boron trifluoride diethyl etherate</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3587191', constants.ctx, '0')">dihydrogen peroxide</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3595639', constants.ctx, '0')">sodium acetate</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '4371014', constants.ctx, '0')">ammonium chloride</a> <br />&nbsp;Yield given. Multistep reaction;&nbsp;<br /> &nbsp;