(4-硝基-吡啶-2-基)-甲醇合成路线 （共 11 条）
反应条件
trifluoroacetic anhydride in dichloromethane T=20°C; 72 h;
参考文献
Comba, Peter; Morgen, Michael; Wadepohl, Hubert
Inorganic Chemistry, 2013 , vol. 52, # 11 p. 6481 - 6501
反应条件
water; sodium hydroxide in methanol 1.5 h; Inert atmosphereReflux;
参考文献
Chen, Hongfeng; Sweet, James A.; Lam, Kin-Chung; Rheingold, Arnold L.; McGrath, Dominic V.
Tetrahedron Asymmetry, 2009 , vol. 20, # 14 p. 1672 - 1682
反应条件
1: 83.9 percent / H2SO4; HNO3 / 2 h / 110 - 115 °C 2: 0.5 h / 110 - 120 °C 3: 1 mol/l aq. NaOH / methanol / 0.75 h / 20 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 48, # 10 p. 1514 - 1518
反应条件
acetic anhydride Erwaermen des Reaktionsprodukts mit wss.Salzsaeure;
参考文献
Yakugaku Zasshi, , vol. 77, p. 11,13
Chem.Abstr., , p. 8745
反应条件
T=110 - 120°C; und Erwaermen des Reaktionsprodukts mit wss. Salzssaeure;
参考文献
Yakugaku Zasshi, , vol. 77, p. 11,13
Chem.Abstr., , p. 8745
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine; p-toluenesulfonyl chloride in dichloromethane T=0 - 15°C; 12.5 h;
参考文献
Ding, Rui; He, Yong; Wang, Xiao; Xu, Jingli; Chen, Yurong; Feng, Man; Qi, Chuanmin
Molecules, 2011 , vol. 16, # 7 p. 5665 - 5673
反应条件
1: selenium(IV) oxide / 1,4-dioxane / 5 h / 85 °C 2: acetyl-bromide / 15 h / 60 - 70 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Comba, Peter; Morgen, Michael; Wadepohl, Hubert
Inorganic Chemistry, 2013 , vol. 52, # 11 p. 6481 - 6501
反应条件
manganese(IV) oxide in dichloromethane T=25°C; 72 h;
参考文献
Zaman, Nicolas; Guillot, Regis; Senechal-David, Katell; Boillot, Marie-Laure
Tetrahedron Letters, 2008 , vol. 49, # 51 p. 7274 - 7275
反应条件
1: ethanol / 24 h / |Reflux 2: selenium(IV) oxide / 1,4-dioxane / 4 h / 90 °C View Scheme
参考文献
Comba, Peter; Morgen, Michael; Wadepohl, Hubert
Inorganic Chemistry, 2013 , vol. 52, # 11 p. 6481 - 6501
反应条件
in methanol T=80°C; 24 h; Reflux;
参考文献
Inorganic Chemistry, , vol. 52, # 11 p. 6481 - 6501
